Food Control Laboratory Analysis List

KONYA FOOD AND AGRICULTURE UNIVERSITY COMMERCIAL ENTERPRISE
SARGEM SPECIAL FOOD CONTROL LABORATORY ANALYSIS LIST

Queue

No

Analysis Name

SOP Code

Product/Product Group Covered by the Method

Original Method Source(s)

Technique Used *

Analysis Type

(Qualitative/

Quantitative)

1

Acidity

AT-GKL-KIM-01/1

Butter

TS 1740

Titrimetric

Quantitative

AT-GKL-KIM-01/2

Edible vegetable and animal oils, extracted oils, Oilseeds

TS EN ISO 660

Titrimetric

Quantitative

AT-GKL-KIM-01/3

Powdered Soft Drink

TS 7058 ATIF TS 1125 ISO

750

Titrimetric

Quantitative

AT-GKL-KIM-01/4

Tarhana

TS 2282

Titrimetric

Quantitative

AT-GKL-KIM-01/5

Starch

TS 2970,TS 4500

Titrimetric

Quantitative

AT-GKL-KIM-01/6

Processed hazelnut kernels

TS 1917,TS EN ISO 660

Titrimetric

Quantitative

AT-GKL-KIM-01/7

Bread

TS 5000

Titrimetric

Quantitative

AT-GKL-KIM-01/8

Bal

TS 13360

Titrimetric

Quantitative

2

Acidity (As Anhydrous Citric Acid)

AT-GKL-KIM-02

Fruit Juice etc. Products

TS 1125 ISO 750

Titrimetric

Quantitative

3

Crude Ash Determination

AT-GKL-KIM-03

Compound Feeds and Feed Raw Materials

MoFAL, Feedstuffs and

Compound Feeds

Composition of

Not to be Checked

Analysis Methods Used

2017/29955 R.G

Gravimetric

Quantitative

4

Determination of Formol Number

AT-GKL-KIM-04

Fruit and Vegetable Juices

TS EN 1133

Titrimetric

Quantitative

5

Free Amino Acid Determination

AT-GKL-KIM-05

Compound Feed, Feed Raw Materials, Food

Articles

Kit Method (Waters Kit Application Note)

Chromatographic

Quantitative

6

Total Sugar (Fructose, Glucose, Sucrose)

AT-GKL-KIM-06

Bal

TS 13359

Chromatographic

Quantitative

7

Homogenization Experiment

AT-GKL-KIM-07

UHT and Pasteurized Milk

TS 1019

Gravimetric

Quantitative

8

Invert Sugar Analysis

AT-GKL-KIM-08

Mulberry Molasses

TS 12001

Titrimetric

Quantitative

9

Sugar Determination

AT-GKL-KIM-09

Compound Feeds and Feed Raw Materials

Food, Agriculture and Livestock

Ministry of Feedstuffs and

Compound Feeds

Composition of

In Controlling

Used

Methods of Analysis Section :H

Titrimetric

Quantitative

10

Starch quantity determination

AT-GKL-KIM-10

Meat Products

TS 6812

Gravimetric

Quantitative

11

Peroxide number

AT-GKL-KIM-11

Edible Vegetable and Animal Oils, Extracted Oils

TS EN/ISO 3960

Titrimetric

Quantitative

12

Polar Sugar (Polarization Value) Determination

AT-GKL-KIM-12

White Sugar

TGK 2006/40

Spectrophotometric

Quantitative

13

Moisture content determination

AT-GKL-KIM-13

Spices, Potato Chips, Turkish Delight

TS 2134, TS 3628, TS 8444

Gravimetric

Quantitative

14

Sugar determination

AT-GKL-KIM-14

Invert sugar syrup glucose syrup

TGK 2002/26

Titrimetric

Quantitative

15

Titration acidity

AT-GKL-KIM-15/1

Pasteurized Milk, Raw Milk, Buttermilk, Cream

TS 1018

Titrimetric

Quantitative

AT-GKL-KIM-15/2

Feta Cheese, Tulum Cheese, Tongue Cheese

TS 591 - AOAC 920.124

Titrimetric

Quantitative

AT-GKL-KIM-15/3

Yogurt

TS 1330

Titrimetric

Quantitative

AT-GKL-KIM-15/4

Milk Powder

TS 1329

Titrimetric

Quantitative

16

Total Sugar Analysis

AT-GKL-KIM-16/1

Biscuits, Tomato Paste, Hazelnut Paste, Soda, Powder Soft Drinks

TS 1466

Titrimetric

Quantitative

AT-GKL-KIM-16/2

Chocolate

TS 7800

Titrimetric

Quantitative

AT-GKL-KIM-16/3

Mulberry Molasses

TS 12001

Titrimetric

Quantitative

AT-GKL-KIM-16/4

Akide Şekeri, Turkish Delight, J öle Şekerleme, Tahini Halva, Ice Cream, Pismaniye, Summer Halva

TS 7780

Titrimetric

Quantitative

17

Salt determination

AT-GKL-KIM-17/1

Butter

TS ISO 1738

Titrimetric

Quantitative

AT-GKL-KIM-17/2

Spices, Potato Chips, Instant Dry

Soups

TS 3190 citation TS 5000

Titrimetric

Quantitative

AT-GKL-KIM-17/3

Bread

TS 5000

Titrimetric

Quantitative

AT-GKL-KIM-17/4

Meat Products

TS 1747 (1999)

Titrimetric

Quantitative

AT-GKL-KIM-17/5

Buttermilk, Cheese Types

TS EN ISO 5943

Titrimetric

Quantitative

AT-GKL-KIM-17/6

Turnip Juice

TS 2664

Titrimetric

Quantitative

AT-GKL-KIM-17/7

Cooking Salt

TS 933

Titrimetric

Quantitative

18

Oil determination

AT-GKL-KIM-18/1

Meat and Meat Products

TS 1744

Gravimetric

Quantitative

AT-GKL-KIM-18/2

Chocolate

TS 7800

Gravimetric

Quantitative

AT-GKL-KIM-18/3

Potato Chips, Instant Dry Soups, Spices, Oil Seeds

TS 2664

Gravimetric

Quantitative

AT-GKL-KIM-18/4

Raw Milk, Pasteurized Milk, Flavored Milk, Buttermilk

TS 2446

Gravimetric

Quantitative

AT-GKL-KIM-18/5

Condensed milk, Milk Powder

TS EN ISO 1736

Gravimetric

Quantitative

AT-GKL-KIM-18/6

Ice cream

TGK 2004/45

Gravimetric

Quantitative

AT-GKL-KIM-18/7

Butter, Spreads, Margarines and

Intensive Oils

TS 1331

Gravimetric

Quantitative

AT-GKL-KIM-18/8

Cream, Cream

TS 1864

Gravimetric

Quantitative

AT-GKL-KIM-18/9

All Cheeses

TS ISO 3433

Gravimetric

Quantitative

AT-GKL-KIM-18/10

Tahini Halva

TS 2590

Gravimetric

Quantitative

AT-GKL-KIM-18/11

Tahini

TS 2589

Gravimetric

Quantitative

AT-GKL-KIM-18/12

Cereals and cereal products

TS EN ISO 11085

Gravimetric

Quantitative

19

Fatty acid composition;

AT-GKL-KIM-19

Vegetable Oils

TS EN IS012966-2:2011

TSE EN ISO 12966-4 OCTOBER 2015

Chromatographic

Quantitative

Arachidic A, Behenic A., Butyric A., DHA, Ecosenoic A., Eruis A., Heptadecanoic A., Capric A., Caprylic A., Caproic A., Lauric A., Lignoceric A., Linoleic A., Linoleinic A., Margaric A., Nevoic A., Myristic A., Oleic A., Palmitic A., Palmitoleic A., Stera,k A,

20

Aflatoxin B1 and

Total Aflatoxin

(B1+B2+G1+G2)

AT-GKL-KIM-20/1

Hazelnuts, Peanuts, Pistachios, Oily Dry Fruits and Products Derived Therefrom

In-house method (modified from AOAC Official Method 999.07.

Chromatographic

Quantitative

21

Aflatoxin B1 and

Total Aflatoxin

(B1+B2+G1+G2)

AT-GKL-KIM-20/2

Figs, Grapes, Red Peppers and Dried Fruits and Products

In-house method (modified from AOAC Official Method 999.07.

Chromatographic

Quantitative

22

Aflatoxin B1 and

Total Aflatoxin

(B1+B2+G1+G2)

AT-GKL-KIM-20/3

Feed, feed raw materials and

high fiber products

In-house method (AOAC

Modified from Official Method 2003.03.

Chromatographic

Quantitative

23

Aflatoxin B1 and

Total Aflatoxin

(B1+B2+G1+G2)

AT-GKL-KIM-20/4

Whole Grains

In-house method (RBiopharm. Aflaprep

Instruction Manual

P07/V19/02.2013 modified)

Chromatographic

Quantitative

24

Patulin Analysis

AT-GKL-KIM-21

Apple Juice, Apple

Concentrates, Applesauce and Drinks Containing Apple Juice

In-house method (R-

Bıopharm Application

Note

p250b/v3/02.12.2013 modified)

Chromatographic

Quantitative

25

Aflatoxin M1 Analysis

AT-GKL-KIM-22

Milk and milk powder

In-house method (ISO

14501 Milk and Milk powder-Determination of aflatoxin M1 content clean up by

immunoaffinity

chromatography and

determination by high performance liquid

chromatography,2007 modified)

Chromatographic

Quantitative

26

Ochratoxin A Analysis

AT-GKL-KIM-23/1

Feed and feed raw materials

In-house method (AOAC

Official Method 2000.03

Ochratoxin A in Barley

Chapter 49, p 65 modified)

Chromatographic

Qualitative

27

Ochratoxin A Analysis

AT-GKL-KIM-23/2

Cereals and cereal products

In-house method (R-

BIOPHARMA Cereal

Application Note Ref

No:A9-P14.V2,December 2001 modified)

Chromatographic

28

Crude Cellulose Determination

AT-GKL-KIM-24

Compound Feeds and Feed Raw Materials

Ministry of Food, Agriculture and Livestock

Feedstuffs and Compound

Composition of Feeds

In Controlling

Methods of Analysis Used Section: EC 152/2009

Gravimetric

Quantitative

29

Starch Determination

AT-GKL-KIM-25

Compound Feed, Feed Raw Materials,

Plant Foods

Food, Agriculture and Livestock

Ministry of Feedstuffs and

Compound Feeds

Composition of

In Controlling

Used

Methods of Analysis Section :I

EC 152/2009 TS EN ISO 10520

Spectrophotometric

Quantitative

30

Protein Determination

AT-GKL-KIM-26

Compound Feeds,

Feed Raw Materials and Whole Foods

AOAC 990.03

AOAC 992.23

Application Dumatherm Note

Chromatographic

Quantitative

31

Crude Oil Determination

AT-GKL-KIM-27

Compound Feeds and Feed Raw Materials

Food, Agriculture and Livestock

Ministry of Feedstuffs and

Compound Feeds

Composition of

In Controlling

Used

Methods of Analysis Section: G EC 152/2009 / Welp

Scientific Ser 148 Manual

Gravimetric

Quantitative

32

Determination of Insoluble Ash in Hydrochloric Acid (HCl)

AT-GKL-KIM-28

Compound Feeds and Feed Raw Materials

Food, Agriculture and Livestock

Ministry of Feedstuffs and

Compound Feeds

Composition of

In Controlling

Used

Methods of Analysis Section K 2017/29955 R.G

Gravimetric

Quantitative

33

Determination of Urease Activity

AT-GKL-KIM-29

Soybean Meal

TS 4707 ISO 5506

Volumetric

Quantitative

34

Weight Determinations (Gross, Net)

AT-GKL-FİZ-01

Canned, strained mass

TGK (76/211/AT), TS 2664

Gravimetric

Quantitative

AT-GKL-FİZ-01

Egg

TGK 2014/55, TS 1068

Gravimetric

Quantitative

AT-GKL-FİZ-01

Bread

TS 5000, 2012/2 Communiqué (Amended 2013/10 Communiqué)

Gravimetric

Quantitative

35

Determination of Acid Insoluble Matter

AT-GKL-PHYS-02

Salt

TS 1346

Gravimetric

Quantitative

36

Electrical Conductivity Determination

AT-GKL-FIZ-03

Bal

TS 13366

Gravimetric

Quantitative

AT-GKL-FIZ-03

Su

TS 9748 EN 27888

Gravimetric

Quantitative

37

Ash Insoluble in Hydrochloric Acid (HCl)

AT-GKL-FİZ-04

Biscuits, Cereals and Grain Products

TS 2383

Gravimetric

Quantitative

AT-GKL-FİZ-04

In black tea

TS 1566 ISO 1577

Gravimetric

Quantitative

AT-GKL-FİZ-04

Cocoa (beans and ground)

TS 3076-1

Gravimetric

Quantitative

AT-GKL-FİZ-04

Spice

TS 2133 ISO 930

Gravimetric

Quantitative

38

Grain Size, Sieve, Coarseness, Grading

AT-GKL-PHYS-05

Edible starch

TS 2970

Gravimetric

Quantitative

AT-GKL-PHYS-05

Cooking salt

TGK 2013/48

Gravimetric

Quantitative

AT-GKL-PHYS-05

Black Tea

TS 4600, TGK tea communiqué 2015/30

Gravimetric

Quantitative

39

Physical Defect Broken Grain

AT-GKL-PHYS-06

Rice

TS 2408, TGK 2010/60

Gravimetric

Quantitative

40

Refractive Index Determination

AT-GKL-FIZ-07

Animal and vegetable oils

TS 4960 EN ISO 6320, TGK NO: 2012/29

Gravimetric

Quantitative

41

Dampness / Humidity, Dry

Substance / Solid Matter

Amount

AT-GKL- PHYS-08

Milk and buttermilk

TS1018:2002

Gravimetric

Quantitative

AT-GKL- PHYS-08

Yogurt

TS1330

Gravimetric

Quantitative

AT-GKL- PHYS-08

Cheese

TS EN ISO 5534

Gravimetric

Quantitative

AT-GKL- PHYS-08

Butter

TS 1331/AOAC 920.116

Gravimetric

Quantitative

AT-GKL- PHYS-08

Ice cream

TS ISO 3728

Gravimetric

Quantitative

AT-GKL- PHYS-08

Milk Powder

TS 1329/AOAC 927.05

Gravimetric

Quantitative

AT-GKL- PHYS-08

Condensed milk

TS 7790

Gravimetric

Quantitative

AT-GKL- PHYS-08

Cream

TS1018:2002

Gravimetric

Quantitative

AT-GKL- PHYS-08

Chocolate

TS 7800

Gravimetric

Quantitative

AT-GKL- PHYS-08

Tea

TS1562

Gravimetric

Quantitative

AT-GKL- PHYS-08

Grains and products, Legumes

TS EN ISO 712

Gravimetric

Quantitative

AT-GKL- PHYS-08

Cooking salt

TS 933/ AOAC 925.55

Gravimetric

Quantitative

AT-GKL- PHYS-08

Bread

TS 5000

Gravimetric

Quantitative

AT-GKL- PHYS-08

Bread yeast

TS 3522

Gravimetric

Quantitative

AT-GKL- PHYS-08

Edible starch

TS 1252 EN ISO 1666

Gravimetric

Quantitative

AT-GKL- PHYS-08

Tahini Halva

TS 1201 EN ISO 1741

Gravimetric

Quantitative

AT-GKL- PHYS-08

Meat and meat products

TS 1743 ISO 1442

Gravimetric

Quantitative

42

Loss on Drying

AT-GKL- PHYS-08

Semi-white sugar, sugar or white sugar, refined sugar

TS 861, Communiqué 2002/26

Gravimetric

Quantitative

43

Ash and Crude Ash Determination

AT-GKL-PHYS-10

Bal

TS3036

Gravimetric

Quantitative

AT-GKL-PHYS-10

Soluble coffee

TS 5389

Gravimetric

Quantitative

AT-GKL-PHYS-10

Cereals, legumes and products

TS EN ISO 2171/AOAC 923.03

Gravimetric

Quantitative

AT-GKL-PHYS-10

Edible casein and caseinates

TGK 2002/18

Gravimetric

Quantitative

AT-GKL-PHYS-10

Black tea

TS 1564

Gravimetric

Quantitative

AT-GKL-PHYS-10

Cocoa (beans and ground)

TS 3076-1

Gravimetric

Quantitative

AT-GKL-PHYS-10

Spice

TS 2131 ISO 928

Gravimetric

Quantitative

AT-GKL-PHYS-10

Molasses

TS 3792

Gravimetric

Quantitative

AT-GKL-PHYS-10

Coffee (beans and ground)

TS 13423

Gravimetric

Quantitative

AT-GKL-PHYS-10

Tahini Halva

TS ISO 6884

Gravimetric

Quantitative

44

Determination of Water Insoluble Solids

AT-GKL-PHYS-11

Bal

TS 3036

Gravimetric

Quantitative

45

pH Determination

AT-GKL-PHYS-12

Meat and meat products

TS 3136 ISO 2917, COMMUNIQUÉ

NO: 2012/74 and amendment

2015/7 and 2015/33

Gravimetric

Quantitative

AT-GKL-PHYS-12

Fruit and vegetable products

TS 1728 ISO 1842

Gravimetric

Quantitative

46

Refractometric Moisture Determination

AT-GKL-PHYS-13

Bal

TS 13365

Gravimetric

Quantitative

47

Density, relative density, specific gravity

AT-GKL-PHYS-14

Animal and Vegetable Oils

TS 4959

Gravimetric

Quantitative

48

Water Solubility Rate

Determination

AT-GKL-PHYS-15

Milk Powder

TS 1329

Gravimetric

Quantitative

49

Determination of Water Soluble Solids

AT-GKL-PHYS-16

Fruit and vegetable products

TS 12143, TS 4890

Gravimetric

Quantitative

50

AEROBIC COLONY COUNT

AT-GKL-MIK-01

Whole foods

FDA chapter 3

Counting Technique

Quantitative

51

AEROBIC COLONY COUNT

AT-GKL-MIK-02

Whole foods

ISO 4833-1

Counting Technique

Quantitative

52

MOLD - YEAST COUNT

AT-GKL-MIK-03

Whole foods

ISO 21527-1, ISO 21527-2

Counting Technique

Quantitative

53

Enterobacteriaceae CENSUS

AT-GKL-MIK-04

Whole foods

ISO 21528-2

Counting Technique

Quantitative

54

COLIFORM (EMS) COUNT

AT-GKL-MIK-05

Whole foods

ISO 4831

EMS

Quantitative

55

COLIFORM (PLATE COUNT)

AT-GKL-MIK-06

Whole foods

ISO 4832

Counting Technique

Quantitative

56

E. coli (EMS) COUNT

AT-GKL-MIK-07

Whole foods

ISO 7251

EMS

Quantitative

57

E. coli (PLATE COUNT)

AT-GKL-MIK-08

Whole foods

ISO 16649-2

Counting Technique

Quantitative

58

COAGULASE POSITIVE

STAPHYLOCOCCI

(Staphylococcus aureus and other species) COUNT

AT-GKL-MIK-09

Whole foods

ISO 6888-1

Counting Technique

Quantitative

59

Bacillus cereus COUNT

AT-GKL-MIK-10

Whole foods

ISO 7932

Counting Technique

Quantitative

60

Salmonella spp.

SEARCH

AT-GKL-MIK-11

Whole foods

ISO 6579

Yes/No

Qualitative

61

Salmonella spp.

SEARCH FOR RAPICHECK

AT-GKL-MIK-12

Whole foods

AOAC 080601

Yes/No

Qualitative

62

Listeria monocytogenes

SEARCH

AT-GKL-MIK-13

Whole foods

ISO 11290-1

Yes/No

Qualitative

63

E. coli O157 H7

SEARCH FOR RAPICHECK

AT-GKL-MIK-14

Meat and Meat Products

AOAC 070801

Yes/No

Qualitative

64

Listeria spp. RAPICHECK

SEARCH

AT-GKL-MIK-15

Meat and Meat Products, Milk and Milk

Products, Fish Products and Various Foods

AOAC 020401

Yes/No

Qualitative

65

E. coli O157 H7

SEARCH

AT-GKL-MIK-16

Whole foods

ISO - 16654

Yes/No

Qualitative

66

Species Determination in Meat and Meat Products (Horse Meat Search)¹

AT-GKL-MIK-17

Meat and Meat Products

Kit Procedure (ELISA-TEK), USDA, Microbiology Lab.

Guide Book Chapter 17,3 Edition (Elisa)

ELISA

Qualitative

67

Type in Meat and Meat Products

Determination (Pork

Search)¹

AT-GKL-MIK-18

Meat and Meat Products

Kit Procedure (ELISA-TEK), USDA, Microbiology Lab.

Guide Book Chapter 17,3 Edition (Elisa)

ELISA

Qualitative